By R. Schöllhorn (auth.), W. Müller-Warmuth, R. Schöllhorn (eds.)

ISBN-10: 940104385X

ISBN-13: 9789401043854

ISBN-10: 9401108900

ISBN-13: 9789401108904

The mix of stable fabrics of alternative structural dimensionality with atomic or molecular visitor species through intercalation strategies represents a different and commonly variable low temperature synthesis approach for the layout of solids with specific composition, constitution and actual houses. within the final decade this box has skilled a fast improvement and represents now a longtime particular area of good kingdom examine and fabrics technology. colossal growth has been made with recognize to an realizing of the advanced courting among constitution, bonding, actual homes and chemical reactivity because the first quantity at the topic seemed during this sequence in 1979 (Intercalated Layered fabrics, F. Levy, ed.). the aim of this quantity is to provide a survey on development and according to­ spectives in accordance with the therapy of a sequence of significant components of actions during this box. via the very nature of its topic this monograph has an interdisciplinary personality and addresses itself to chemists, physicists and fabrics scien­ tists attracted to intercalation study and comparable points akin to layout and characterization of complicated fabrics, low temperature synthesis, stable nation response mechanisms, electronic/ionic conductivity, keep watch over of digital houses of solids with diverse structural dimensionality and alertness of intercalation structures. numerous chapters were dedicated to particular teams of host lattices.

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This possibility has been demonstrated for the intercalation of polyoxyethylene into montmorillonite and V20S gels; there is evidence that the guest polymer prefers a helical arrangement in the interlamellar space [264, 265]. A stimulating review concerning these and related materials is found in reference [266]. 9. CHARACTERIZATION Intercalation chemistry is a domain of solid state chemistry and all available techniques for the characterization of solids are applicable of course to the MATERIALS AND MODELS: FACES OF INTERCALATION CHEMISTRY 39 Fig.

000 000000 000000 000000 000000 000000 ""'000 ""'0000 Fig. 26. Staging transitions in layered intercalation systems. (a) simple model, (b) domain model after Herold-Daumas. 27. The diffractograms can be interpreted on grounds of simulations by the Hendrixffeller formalism [300] (Figure 27c) in terms of statistical mixtures of intercalated and non intercalated regions with different volume ratio although the reflection intensities have not been taken into account. For small ions like Li+ staging intermediates have so far only been reported for the system Lix[SnS2] [301].

It is obvious that only a few representatives of the large variety of compounds with channel structures have been studied with respect to intercalation processes. 4. Layered Chalcogenide Phases As mentioned already above layered transition metal dichalcogenides MX2 have traditionally been a 'test field' for materials and models in intercalation chemistry due to their simple layer structures, the variability in host lattice composition by isomorphous substitution of M and X, the wide range of potential guest species due to the flexibility of the layered systems and due to the range in interesting low dimensional physical properties and the possibility to control the latter via redox intercalation reactions.

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Progress in Intercalation Research by R. Schöllhorn (auth.), W. Müller-Warmuth, R. Schöllhorn (eds.)


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